Welcome to Precision Petroleum Lab

5915 Star Lane

Houston, Texas 77057

(713) 680-9425

TESTING FORMS USED BY PRECISION PETROLEUM LABS

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Summary Guide to Lab Requirements:

Virgin Contaminants
Contaminant	NH	NY
Gasoline / Jet Fuel	- TPH-GRO - Total Lead ¹	- TPH-GRO ⁴ - Total Lead ¹
#2 Fuel Oil Diesel	- TPH-DRO ² - Total Lead ¹	- TPH-DRO^3,4 - Total Lead ¹
#4, 6 Fuel Oil	-TPH-DRO² -Total lead¹ -Total VOCs⁹ -Total SVOCs⁹	- TPH-DRO^3,4 - Total Lead ¹
Mixed Fuels (fuel oil /gas)	- TPH-DRO/GRO - Total Lead ¹	- TPH-DRO/GRO ⁴ - Total Lead ¹
Animal, Vegetable, Tall oil	- TPH by 8100 or 8015DRO	- TPH by 8100 or 8015DRO ⁴
Petroleum Solvents	- TPH by 8100 or 8015DRO - Total VOC’s - Total SVOC’s - Ignitibility/Flash	- TPH by 8100 or 8015DRO ⁴ - Total VOC’s ⁴ - Total SVOC’s ⁴
Waxes and Petrolatum	- TPH by 8100 or 8015DRO - Total VOC’s - Total SVOC’s	- TPH by 8100 or 8015DRO ⁴ - Total VOC’s ⁴ - Total SVOC’s ⁴

Non-Virgin Contaminants
Contaminant	NH	NY
Used Oils, Greases, Lubricants	- TPH by 8100 or 8015DRO - Total VOC’s - Total RCRA 8 metals	- TPH by 8100 or 8015DRO - Total VOC’s - Total RCRA 8 metals
Used Animal, Vegetable, Tall oils	- TPH by 8100 or 8015DRO - Total VOC’s - Total SVOC’s - Total RCRA 8 metals	- TPH by 8100 or 8015DRO
Petroleum Solvents (used)	- TPH by 8100 or 8015DRO - Total VOC’s - Total SVOC’s - Total RCRA 8 metals - Ignitibility/Flash	- TPH by 8100 or 8015DRO - Total VOC’s - Total SVOC’s - Total RCRA 8 metals - Ignitibility/Flash

Coal Tars / PCBS / Urban Fill
Contaminant	NH	NY
Coal tars, coal, pitch, tar, asphalt emulsion	- TPH by 8100 or 8015DRO - Total VOC’s - Total SVOC’s - Total RCRA 8 metals - Total Cyanide / %Sulfur ( Non-Reactive	- TPH by 8100 or 8015DRO - Total VOC’s - Total SVOC’s - Total RCRA 8 metals - Total Cyanide / %Sulfur - Total BTU - Total PCBs
Urban Fill	- TPH by 8100 or 8015DRO - Total VOC’s - Total PAH's - Total RCRA 8 metals - PCBs	- TPH by 8100 or 8015DRO - Total VOC’s - Total SVOC’s - Total RCRA 8 metals - PCBs
Electrical oils	- TPH-DRO - Total PCBs	- TPH-DRO - Total PCBs,
Transformer Oils	- TPH-DRO - Total PCBs	- TPH-DRO - Total PCBs
Dredge ⁶	- TPH by 8100 or 8015DRO - Total VOC’s - Total PAH's - Total RCRA 8 metals - PCBs - Total Cyanide / %Sulfur ⁵	- TPH by 8100 or 8015DRO - Total VOC’s - Total SVOC’s - Total RCRA 8 metals - Total Cyanide / %Sulfur⁵ - Total BTU ⁵ - Total PCBs

Notes:

1) Total lead required for urban areas, and historical gas releases where lead may have been present.

2) (NH Facility): Virgin Fuel Releases less than 50 tons do not require sampling as long as the generator certifies that there are no other contaminants present.

3) (NY Facility): Certified residential sites under 150 tons require in-house TPH testing only.

4) (NY Facility): NYSDEC directed virgin spill cleanups require in-house TPH when
certified virgin and characterization is waived by a NYSDEC Spill Representative.

5) Required if coal tar is present.

6) Dredged soil must be sampled prior to mixing or drying. Chain of Custody must reflect this and be included with all lab results.

7) Any soils containing a listed hazardous waste, may be accepted, at the discretion of the facility when accompanied with a State Certified “contained-out” determination.

8) At the discretion of the facility, additional lab may be required for project acceptance.

9) One sample required for each 500 tons.

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4. Acceptable Lab Methods:

All analysis is required to be conducted by a State Certified lab using SW-846 Methods*.

Analysis	Method
TPH	GC/FID
Total VOC's	Method 8260
Total SVOC's / PAH	Method 8270
RCRA 8 Metals	Method 6010B ( Arsenic, Barium, Cadmium, Chromium Total, Lead, Selenium, Silver and Mercury (7471A) )
PCBs	Method 8082
Ignitibility	Method 1010
Total Cyanide	Method 9010
Total Sulfur	EPA D129-64
BTU	ASTM-D240-87

Sample	ESMI of NH	Sum of Tons NH	ESMI of NY	Sum of Tons NY
1st Sample	200 Tons	200	150 Tons	150
2nd Sample	200 Tons	400	150 Tons	300
3rd Sample	200 Tons	600	450 Tons	750
4th Sample	200 Tons	800	750 Tons	1500
5th Sample +	Each Sample is equal to 200 tons, up to 4000 tons (20 samples) then 500 tons after that.	1000 and up	Each additional sample is worth 750 tons	2250

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Scheduling soil to the facility:

Once the waste has been properly profiled and laboratory data has been reviewed and approved by the Precision Petroleum Labs compliance department, the job can be scheduled through the sales department. We encourage customers to communicate their needs as far out as possible and keep us informed of any changes. We want your project to run as smoothly as you do, the more involved we get in the work schedule the better we can serve your needs.

Required Shipping Papers
State	Shipping Papers
New Hampshire	Straight BOL or Non-hazardous waste manifest
Massachusetts	Mass BOL, MSR or Non-hazardous waste manifest
New York	Straight BOL or Non-hazardous waste manifest
Vermont	Straight BOL or Non-hazardous waste manifest
Maine	Straight BOL or Non-hazardous waste manifest
Connecticut	Straight BOL or Non-hazardous waste manifest

(Note: Some special situations may exist where other documents are required on a case by case basis)

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